Gluing Tests - DIPTEM Genova - Adhesives Shear tests with four different adhesive types: Adhesive tape Adhesive tape Liquid glue Adhesive film NITTO DENKO 30 µm thick 3M 9461P – 30 µm thick Araldite 2020 FastelFilm 30 µm thick • • Polyester film double coated by acrylic adhesive Polyester = 0.13-0.15 W/m K Acrilyc = 0.2 W/m K • 3M Adhesive 100 (Acrylic adhesive) 3M Adhesive 100 = 0.178 W/m K • • • ⁻ ⁻ ⁻ Surface cleaning with acetone 1 Kg for 65 hours ⁻ ⁻ Surface cleaning with acetone 1 Kg for 65 hours ⁻ ⁻ Two components epoxy liquid glue Epoxy = 0.188 W/m K Surface cleaning with acetone Vacuum outgassing after mixing the component Dispensing with a slice • • - EVA (Ethylene - vinyl Acetate) adhesive film EVA = 0.34 W/m K Surface cleaning with acetone 1 Kg for 3 minutes 80 °C in the oven (weight and plate already hot) Gluing Tests - DIPTEM Genova - Samples Silicon samples 10 x 10 mm Silicon glue Silicon Araldite: 10 samples + 2 FastelFilm: 10 samples + 4 (2 with the weight 2 without) NittoDenko: 10 samples + 4 (2 with the weight 2 without) 3M: 10 samples + 4 (2 with the weight 2 without) - TEST of Jerome’s tool: 3 samples glued with NittoDenko double tape - 2 samples per glue type tested (with or without 1 kg weight) - 5 samples per glue type to be ‘natural’ tested - 5 samples per glue type to be tested after irradiation Gluing Tests - DIPTEM Genova - Machine INSTRON 8802 – Floor Model Fatigue Testing Systems up to 500 kN Top clamp Bottom clamp Gluing Tests - DIPTEM Genova - Results Preliminary test of the tool 1 2 3 01 Nitto 02 Nitto 03 Nitto Larghezza (mm) 10,00000 10,00000 10,00000 1 2 3 Velocità di prova (mm/min) 1,30000 1,30000 1,30000 Forza massima (N) 140,73849 116,31846 163,82933 Etichetta provino Spessore (mm) 10,00000 10,00000 10,00000 Carico massimo (MPa) 1,407 1,163 1,638 Gluing Tests - DIPTEM Genova - Results 5 Gluing Tests - DIPTEM Genova - Results 6 Gluing Tests - DIPTEM Genova - Results S1 and S2 = without weight of 1 kg on top S1 and S2 = without weight of 1 kg on top 7 Gluing Tests - DIPTEM Genova - Results S1 and S2 = without weight of 1 kg on top 8 Gluing Tests - DIPTEM Genova - Results Etichetta provino 1 2 3 4 5 6 7 8 9 10 11 12 Nitto S1 Nitto S2 Nitto C1 Nitto C2 3M 1 3M 2 3M S1 3M S2 FF 1 FF 2 FF S1 FF S2 Larghezza (mm) 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 Spessore (mm) 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 10,00000 Velocità di prova (mm/min) 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 1,30000 Forza massima (N) 254,05884 184,07106 242,53726 232,54156 419,92068 503,73673 339,91337 382,59029 459,22995 430,31573 546,66996 413,29265 Gluing Tests - DIPTEM Genova - Results Etichetta provino 13 A1 Larghezza (mm) 10,00000 Spessore (mm) 10,00000 Velocità di prova (mm/min) 1,30000 Forza massima (N) 1706,08759